Stress corrosion cracking of high-pressure gas transmission pipelines
In: Materials & Design, Band 1, Heft 2, S. 80-96
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In: Materials & Design, Band 1, Heft 2, S. 80-96
The structural and vibrational properties of bismuth selenide (Bi 2Se 3) have been studied by means of x-ray diffraction and Raman scattering measurements up to 20 and 30 GPa, respectively. The measurements have been complemented with ab initio total-energy and lattice dynamics calculations. Our experimental results evidence a phase transition from the low-pressure rhombohedral (R-3m) phase (¿-Bi 2Se 3) with sixfold coordination for Bi to a monoclinic C2/m structure (ß-Bi 2Se 3) with sevenfold coordination for Bi above 10 GPa. The equation of state and the pressure dependence of the lattice parameters and volume of ¿ and ß phases of Bi 2Se 3 are reported. Furthermore, the presence of a pressure-induced electronic topological phase transition in ¿-Bi 2Se 3 is discussed. Raman measurements evidence that Bi 2Se 3 undergoes two additional phase transitions around 20 and 28 GPa, likely toward a monoclinic C2/c and a disordered body-centered cubic structure with 8-fold and 9- or 10-fold coordination, respectively. These two high-pressure structures are the same as those recently found at high pressures in Bi 2Te 3 and Sb 2Te 3. On pressure release, Bi 2Se 3 reverts to the original rhombohedral phase after considerable hysteresis. Symmetries, frequencies, and pressure coefficients of the Raman and infrared modes in the different phases are reported and discussed. © 2011 American Physical Society. ; This work was done under financial support from Spanish Ministry of Science and Innovation under Projects No. MAT2007-66129, No. MAT2010-21270-C04-03/04, and No. CSD-2007-00045 and from the Valencian government under Project No. Prometeo/2011-035. It is also supported by the Ministry of Education, Youth and Sports of the Czech Republic Project No. MSM 0021627501. E.P.G. acknowledges the financial support of the Spanish Ministry of Education. Supercomputer time was provided by the Red Espanola de Supercomputacion and the MALTA cluster. ; Vilaplana Cerda, RI.; Santamaría-Pérez, D.; Gomis Hilario, O.; Manjón Herrera, FJ.; ...
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In: Springer eBook Collection
High pressure and High pressure environments -- High pressure: molecules, chemical processes and cellular structures -- The high pressure micro-environment of vertebrate load bearing joints- Effects of high pressure on the activity of ordinary animals, including humans, and on the function of their excitable cells and ion channels -- The effects of decompression and subsequent re-compression on the activity of deep sea animals and eukaryote cells. The isobaric collection of deep sea animals.-Molecular adaptation to high pressure: proteins in deep sea animals -- Molecular adaptation to high pressure: membranes -- Prokaryotes at high pressure in the Oceans and the Deep Biosphere -- Hydrothermal vents: the inhabitants, their way of life and their adaptation to high pressure -- Buoyancy at depth -- Divers: Air breathing animals, including humans, at high pressure -- Adaptation to high pressure in the laboratory -- High pressure equipment used in the laboratory, at sea and at depth.
In: MTZ worldwide, Band 81, Heft 11, S. 56-61
ISSN: 2192-9114
In: Zeitschrift für Metallkunde, Band 96, Heft 10, S. 1211-1212
In: International Geology Review, Band 12, Heft 10, S. 1225-1226
The structural and vibrational properties of bismuth selenide (Bi2Se3) have been studied by means of x-ray diffraction and Raman scattering measurements up to 20 and 30 GPa, respectively. The measurements have been complemented with ab initio total-energy and lattice dynamics calculations. Our experimental results evidence a phase transition from the low-pressure rhombohedral (R-3m) phase (B-Bi2Se3) with sixfold coordination for Bi to a monoclinic C2/m structure (B-Bi2Se3) with sevenfold coordination for Bi above 10 GPa. The equation of state and the pressure dependence of the lattice parameters and volume of a and B phases of Bi2Se3 are reported. Furthermore, the presence of a pressure-induced electronic topological phase transition in B-Bi2Se3 is discussed. Raman measurements evidence that Bi2Se3 undergoes two additional phase transitions around 20 and 28 GPa, likely toward a monoclinic C2/c and a disordered body-centered cubic structure with 8-fold and 9- or 10-fold coordination, respectively. These two high-pressure structures are the same as those recently found at high pressures in Bi2Te3 and Sb2Te3. On pressure release, Bi2Se3 reverts to the original rhombohedral phase after considerable hysteresis. Symmetries, frequencies, and pressure coefficients of the Raman and infrared modes in the different phases are reported and discussed. ; This work was done under financial support from Spanish Ministry of Science and Innovation under Projects No. MAT2007-66129, No. MAT2010-21270-C04-03/04, and No. CSD-2007-00045 and from the Valencian government under Project No. Prometeo/2011-035. It is also supported by the Ministry of Education, Youth and Sports of the Czech Republic Project No. MSM 0021627501.
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In: MTZ worldwide, Band 84, Heft 5, S. 42-47
ISSN: 2192-9114
In: MTZ worldwide, Band 74, Heft 12, S. 62-68
ISSN: 2192-9114
In: Evolution of the Earth and Planets; Geophysical Monograph Series, S. 19-25
In: Research Report or Occasional Paper, 213
In: Working Paper Series, 3
World Affairs Online
This document is the Accepted Manuscript version of a Published Work that appeared in final form in Inorganic Chemistry, copyright © American Chemical Society after peer review and technical editing by the publisher. To access the final edited and published work see http://doi.org/10.1021/acs.inorgchem.8b00778 ; [EN] alpha(R)-In2Se3 has been experimentally and theoretically studied under compression at room temperature by means of X-ray diffraction and Raman scattering measurements as well as by ab initio total-energy and lattice-dynamics calculations. Our study has confirmed the alpha (R3m) -> beta' (C2/m) ? beta (R (3) over barm) sequence of pressure-induced phase transitions and has allowed us to understand the mechanism of the monoclinic C2/m to rhombohedral R (3) over barm phase transition. The monoclinic C2/m phase enhances its symmetry gradually until a complete transformation to the rhombohedral R (3) over barm structure is attained above 10-12 GPa. The second-order character of this transition is the reason for the discordance in previous measurements. The comparison of Raman measurements and lattice-dynamics calculations has allowed us to tentatively assign most of the Raman-active modes of the three phases. The comparison of experimental results and simulations has helped to distinguish between the different phases of In2Se3 and resolve current controversies. ; The authors acknowledge financial support from Spanish government MINECO, the Spanish Agencia Estatal de Investigacion (AEI), and Fondo Europeo de Desarrollo Regional (FEDER) under Grants No. MAT2016-75586-C4-1/2/3-P and MAT2015-71070-REDC. ; Vilaplana Cerda, RI.; Gallego-Parra, S.; Jorge-Montero, A.; Rodríguez-Hernández, P.; Muñoz, A.; Errandonea, D.; Segura, A. (2018). Experimental and Theoretical Studies on alfa-In2Se3 at High Pressure. Inorganic Chemistry. 57:8241-8252. https://doi.org/10.1021/acs.inorgchem.8b00778 ; S ; 8241 ; 8252 ; 57
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In: JMADE-D-21-04310
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The structural and magnetic properties of siderite FeCO3 have been studied by means of neutron powder diffraction at pressures up to 7.5 GPa and first-principles theoretical calculations. The lattice compression in the rhombohedral calcite-type structure is dominated by the reduction of the Fe-O bonds, while the changes of the C-O bonds are much less pronounced. The Neel temperature of the antiferromagnetic ( AFM) ground state increases substantially under pressure with a coefficient dT(N)/dP = 1.8K/GPa, which is about 1.5 times larger in comparison with those predicted by the empirical Bloch rule. The ab initio calculations were performed in the framework of the density functional theory including Hubbard-U correction. The calculated structural parameters and Neel temperature as functions of pressure provide a reasonable agreement with the experimental results. The analysis of the density of electronic states points toward increased covalent bonding between the Fe and O atoms upon pressure, giving rise to unexpectedly large pressure coefficient of the Neel temperature and reduced ordered magnetic moments of Fe atoms. ; Funding Agencies|Ministry of Education and Science of the Russian Federation [14.Y26.31.0005]; Swedish Research Council [2015-04391]; Swedish Government Strategic Research Area in Materials Science on Functional Materials at Linkping University [2009 00971]
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Various applications of transition metal dichalcogenides (TMDs) require preparation by exfoliation of precursor bulk materials. However, bulk TMDs are not always available in suitable forms and current synthesis methods may not result in appropriate crystals. This study reports synthesis of large crystals (50–100 μm) of MoS2 and ReS2, by recrystallisation of MoS2 powder or reaction of sulfate with perrhenic acid, respectively. The reactions have been performed at high pressure and temperature (≥1 GPa; ≥800 °C) in a liquid Ca-carbonate flux. The resulting crystals were characterised by electron microscopy imaging, EDS and WDS chemical analyses, and Raman spectroscopy. The carbonate matrix can be easily dissolved to recover the product TMDs. This method allows synthesis of large well-crystalline TMD compositions that are otherwise challenging to obtain. ; This research is supported by an Australian Government Research Training Program Scholarship and a Ringwood Scholarship. This work was supported by Australian Research Council grant FL130100066 to Hugh O'Neill who provided constructive comments on the manuscript.
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