Mechanical property of cylindrical sandwich shell with gradient core of entangled wire mesh
In: Defence Technology, Band 31, S. 510-522
ISSN: 2214-9147
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In: Defence Technology, Band 31, S. 510-522
ISSN: 2214-9147
In: Materials and design, Band 198, S. 109322
ISSN: 1873-4197
In: Defence Technology, Band 31, S. 557-566
ISSN: 2214-9147
In: Materials and design, Band 213, S. 110333
ISSN: 1873-4197
In: Materials & Design, Band 30, Heft 6, S. 2237-2242
In: Materials & Design, Band 35, S. 120-125
In: Materials & Design, Band 31, Heft 1, S. 574-582
In: Materials & Design, Band 39, S. 131-139
STATEMENT OF PROBLEM. Recently Yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) has been introduced due to superior flexural strength and fracture toughness compared to other dental ceramic systems. Although zirconia has outstanding mechanical properties, the phenomenon of decrease in the life-time of zirconia resulted from degradation in flexural strength after low temperature aging has been reported. PURPOSE. The objective of this study was to investigate degradation of flexural strength of Y-TZP ceramics after various low temperature aging treatments and to evaluate the phase stability and micro-structural change after aging by using X-ray diffraction analysis and a scanning electron microscope (SEM). MATERIAL AND METHODS. Y-TZP blocks of Vita In-Ceram YZ (Vita Zahnfabrik, Bad Sa ¨ckingen, Germany) were prepared in 40 mm (length) x 4 mm (width) x 3 mm (height) samples. Specimens were artificially aged in distilled water by heattreatment at a temperature of 75, 100, 125, 150, 175, 200, and 225℃ for 10 hours, in order to induce the phase transformation at the surface. To measure the mechanical property, the specimens were subjected to a four-point bending test using a universal testing machine (Instron model 3365; Instron, Canton, Mass, USA). In addition, X-ray diffraction analysis (DMAX 2500; Rigaku, Tokyo, Japan) and SEM (Hitachi s4700; Jeol Ltd, Tokyo, Japan) were performed to estimate the phase transformation. The statistical analysis was done using SAS 9.1.3 (SAS institute, USA). The flexural strength data of the experimental groups were analyzed by one-way analysis of variance and to detect statistically significant differences (α= .05). RESULTS. The mean flexural strength of sintered Vita In-Ceram YZ without autoclaving was 798 MPa. When applied aging temperature at below 125℃ for 10 hours, the flexural strength of Vita In-Ceram YZ increased up to 1,161 MPa. However, at above 150℃, the flexural strength started to decrease. Although low temperature aging caused the tetragonal-to-monoclinic phase transformation related to temperature, the minimum flexural strength was above 700 MPa. CONCLUSION. The monoclinic phase started to appear after aging treatment above 100℃. With the higher aging temperature, the fraction of monoclinic phase increased. The ratio of monoclinic/tetragonal + monoclinic phase reached a plateau value, circa 75% above 175℃. The point of monoclinic concentration at which the flexural strength begins to decrease was between 12% and 54%. ; This work was supported by the Korea Science and Engineering Foundation (KOSEF) grant funded by the Korea government(MOST) (No. R01-2007-000-10977-0).
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In: Materials & Design, Band 53, S. 504-511
In: Materials & Design (1980-2015), Band 31, Heft 5, S. 2599-2603
In: Materials and design, Band 241, S. 112959
ISSN: 1873-4197
In: Environmental science and pollution research: ESPR, Band 29, Heft 19, S. 28572-28587
ISSN: 1614-7499
In: Materials & Design, Band 34, S. 655-659
In: Materials and design, Band 132, S. 158-169
ISSN: 1873-4197